Centro de Território, Ambiente e Construção
Escola de Engenharia da Universidade do Minho
Campus de Azurém
4800-058 Guimarães, Portugal
Phone: + 351 253 510 200 (517 206)
Fax: + 351 253 510 217
Email: geral@ctac.uminho.pt
@JournalArticle {3054, title = {Mineralogical and chemical investigation of Tunisian phosphate washing waste during calcination}, journal = {Journal of Thermal Analysis and Calorimetry}, volume = {137}, year = {2019}, month = {2019-10-01 00:00:00}, pages = {1827 - 1840}, publisher = {Springer International Publishing}, abstract = {Phosphate washing waste (PWW) is one of the wastes generated by the phosphate mine with a very high amount. This waste was investigated in this work to study the effect of the calcination of the PWW at four different temperatures 600 oC, 700 oC, 800 oC and 900 oC on its mineralogical and chemical composition. The samples were investigated by X-ray powder diffraction, Fourier transform infrared, differential scanning calorimetry and thermogravimetric analysis, solidstate magic angle spinning nuclear magnetic resonance of 29Si, 27Al and 31P and scanning electron microscope. The results show that the PWW presents a complex system and it suffers a significant change on its mineralogical and chemical composition after calcination. It reveals the presence of carbonate, natural zeolite, fluorapatite, quartz and clay. After calcination, the waste shows the disappearance of some of these phases and the appearance of others and some other phases remain steady.
}, keywords = {Calcination, DSC{\textendash}TG, FTIR, MAS-NMR., Mineralogy, Phosphate washing waste, XRD}, issn = {Print ISSN 1388-6150 | Online ISSN 1588-2926}, doi = {10.1007/s10973-019-08057-3}, author = {Dabbebi, R. and Aguiar, J. B. and Samet, B. and s. Baklouti} }
The Centre for Territory, Environment and Construction (CTAC) is a research unit of the School of Engineering of University of Minho (UMinho), recognised by the “FCT – Fundação para a Ciência e Tecnologia” (Foundation for Science and Technology), associated to the Department of Civil Engineering (DEC), with whom it shares resources and namely human resources.
Currently CTAC aggregates 25 researchers holding a PhD of which 20 are faculty professors of the Civil Engineering Department. Read more
Centro de Território, Ambiente e Construção
Escola de Engenharia da Universidade do Minho
Campus de Azurém
4800-058 Guimarães, Portugal
Phone: + 351 253 510 200 (517 206)
Fax: + 351 253 510 217
Email: geral@ctac.uminho.pt